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Licensee MDPI, Basel, Switzerland. The innovation of the new psychoactive substances (NPS) market requires the speedy identification of latest substances that generally is a threat to public health, so as to reduce the injury from their use. Twelve seized merchandise suspected to contain illicit substances were analyzed by attenuated whole reflectance Fourier transform infrared spectroscopy (ATR-FTIR), gas chromatography coupled to mass spectrometry (GC-MS), and nuclear magnetic resonance spectroscopy (NMR). Synthetic cathinones (SCat) had been found in all products, either as a single element or in mixtures. C) and bands with relative low depth at frequencies near 2700-2400 cm−1, corresponding to an amine salt. It was potential to establish a complete of eight cathinone derivatives by GC-MS and NMR analysis: 4′-methyl-α-pyrrolidinohexanophenone (MPHP), α-pyrrolidinohexanophenone (α-PHP), 3-fluoromethcathinone (3-FMC), methedrone, methylone, buphedrone, N-ethylcathinone, and pentedrone. Among the adulterants found in these samples, caffeine was the most frequently detected substance, followed by ethylphenidate. These outcomes spotlight the prevalence of SCat in seized materials of the Portuguese market.

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Trifluoroacetic anhydride (TFAA ≥ 99.0%), maleic acid (99.0%), trifluoroacetic acid (TFA, 99.0%) and deuterium oxide (99.9%) have been obtained from Sigma-Aldrich (St. Louis, MO, USA), whereas pure caffeine was purchased from Merck (Darmstadt, Germany). Twelve seized merchandise suspected to include illicit substances had been offered by the Forensic Science Laboratory of Portuguese Criminal Police, below a special authorization. The merchandise had been introduced in numerous forms, including powders, crystals and tablets, packed in small plastic baggage with placing designs or, occasionally, in clear plastic luggage. Among the products had been labelled as "plant feeders" with the indication "not for human consumption". Table 1 shows the listing of offered substances, with the respective information about their composition indicated on the product label. A PerkinElmer® Spectrum Two FTIR Spectrometer (Waltham, MA, USA) outfitted with a DuraSamplIR™ diamond ATR unit (Smiths Detection, London, UK) was used for infrared spectroscopy analysis. Approximately 20 mg of powder sample was positioned on the small ATR crystal area, and the infrared spectra have been collected within the vary from 4000 to 600 cm−1, with 32 scans at 4 cm−1 resolution.

Together with, but not restricted to, CP 47,497 (and homologues), cannabicyclohexanol, CP-55, 940. g. Benzoylindoles. Any compound containing a 3-(benzoyl)indole construction with substitution at the nitrogen atom of the indole ring by an alkyl, haloalkyl, alkenyl, cycloalkylmethyl, cycloalkylethyl, 1-(N-methyl-2-piperidinyl)methyl, or 2-(4-morpholinyl)ethyl group, whether or not or not further substituted in the indole ring to any extent and whether or not or not substituted within the phenyl ring to any extent. Together with, but not limited to, AM-694, Pravadoline (WIN 48,098), RCS-4, AM-630, AM-1241, AM-2233. 1-napthalenylmethanone (WIN 55,212-2). i. 1-ol 7370 (HU-210, HU-211). Adamantoylindoles. Any compound containing a 3-(1-adamantoyl)indole structure with substitution on the nitrogen atom of the indole ring by a alkyl, haloalkyl, alkenyl, cycloalkylmethyl, cycloalkylethyl, 1-(N-methyl-2-piperidinyl)methyl or 2-(4-morpholinyl)ethyl group, whether or not further substituted within the indole ring to any extent and whether or not or not substituted in the adamantyl ring system to any extent. 1,9-diol (HU-243, Canbisol). m. 5-pentyl-2,5-cyclohexadiene-1,4-dione (HU-331). n. Indazole-3-carboxamides. Any compound containing an Indazole-3-carboxamide construction with substitution on the nitrogen atom of the indazole ring by alkyl, haloalkyl, halobenzyl, alkenyl, cycloalkylmethyl, cycloalkylethyl, (1-(N-methyl-2-piperidinyl)methyl, (tetrahydro-2H-pyran-4- yl)methyl or (morpholinyl) ethyl group, whether or not further substituted within the indole ring to any extent.